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Go Back   APUG > APUG English Forums > Darkroom > Silver Gelatin Based Emulsion Making & Coating > A peek under the hood

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Old 06-22-2008, 07:23 PM   #1 (permalink)
 
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Default A peek under the hood

I was minding my own business when the doorbell rang and there was this kindly old gentleman with a pushcart on the porch. He asked me if I needed any knives sharpened or umbrellas fixed, and I didn't but I did ask him if he could do electron micrographs.

Lo and behold, he whipped an EM out of his pushcart and said let me at it, so I did.

Here is the result. It is a PM of my SRAD camera speed emulsion, mentioned elsewhere. It is a variant that I'm developing for high speed fine grain applications.

As you see, it is about a 1 micron grain, rather monodisperse and consists of what I would describe as "rounded octahedra". It is just what I wanted to make and now I know exactly where I am and where I have been. I also know where to go next.

So thanks to this kindly guy for doing it for me. He got away before I could get him to do more, but hopefully he will be back someday.

My wife said that this looks like a convention of marshmallows.

PE
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File Type: jpg Electron micrograph - BrI SRAD.jpg (86.9 KB, 165 views)
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Old 06-22-2008, 07:36 PM   #2 (permalink)
 
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octahedra?
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Old 06-22-2008, 08:02 PM   #3 (permalink)
 
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Very cool Ron. Kudos.
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Old 06-22-2008, 08:13 PM   #4 (permalink)
 
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Quote:
Originally Posted by rob champagne View Post
octahedra?
As in octagonal?

http://www.google.com/search?hl=en&q=octahedron

PE
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Old 06-22-2008, 09:35 PM   #5 (permalink)
 
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Must be me then because I can see 6 angles round the edge which gives six faces and what looks like a top face which gives 7 faces on the visible side and assuming that is mirrored on the non visible side, then that would give 14 faces. An Octahedron only has 8 faces.
On the other hand you may just be having another senior moment.

Nice pic though...
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Old 06-22-2008, 10:14 PM   #6 (permalink)
 
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Rob;

Try this and see if it fits: http://en.wikipedia.org/wiki/Truncated_octahedron This as 14 faces.

Nothing is perfect.

PE
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Old 06-22-2008, 10:23 PM   #7 (permalink)
 
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Thats better...
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Old 06-22-2008, 11:21 PM   #8 (permalink)
 
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PE,

This is very interesting. We can use photos like these as an example of what we could expect when building our emulsions.

Thanks,

Bob M.
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Old 06-22-2008, 11:21 PM   #9 (permalink)
 
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Nicely done.

Cheers,
Clarence
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Old 06-22-2008, 11:23 PM   #10 (permalink)
 
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Yes, but was the EM also made on film?
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